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Dual Imaging - a New Frontier in MRI (Interview with Dr. Ashok Ajoy)

MetadataDetails
Publication Date2022-04-11
JournalBerkeley Scientific Journal
AuthorsAndrew Delaney, Lexie Ewer, Esther Lim
InstitutionsBerkeley College, University of California, Berkeley
AnalysisFull AI Review Included

Dual Imaging: A New Frontier in MRI - Technical Analysis and 6CCVD Solutions

Section titled “Dual Imaging: A New Frontier in MRI - Technical Analysis and 6CCVD Solutions”

This research highlights the revolutionary potential of using MPCVD diamond microparticles containing Nitrogen Vacancy (NV) centers to achieve “dual-mode imaging,” significantly enhancing Magnetic Resonance Imaging (MRI) capabilities for biological and physical sciences.

  • Core Value Proposition: Utilizing laser-assisted hyperpolarization of 13C nuclear spins in diamond to overcome the fundamental sensitivity and resolution limits of conventional MRI.
  • Key Achievement: Demonstrated simultaneous high-resolution optical imaging (via NV fluorescence) and high-sensitivity 13C MRI, enabling background-free visualization of diamond particles.
  • Performance Gain: Hyperpolarization resulted in a signal increase up to a million times greater than alignment achieved using standard magnetic fields (1.5 T to 7 T).
  • Mechanism: NV centers act as spin-photon couplers, transferring polarization from absorbed laser light to neighboring 13C nuclei, which are then detected by MRI.
  • Application Focus: Developing quantum-enhanced NMR/MRI technologies for deep tissue imaging, molecular sensing, and early cancer detection.
  • Material Requirement: High-quality, isotopically enriched 13C diamond material with precisely controlled NV defect concentrations is essential for maximizing polarization efficiency and coherence time.

The following table extracts key performance metrics and experimental parameters relevant to the hyperpolarization and imaging techniques discussed.

ParameterValueUnitContext
Polarization EnhancementMillion-foldRatioCompared to normal magnetic field alignment
Polarization Field (Bpol)38 - 40mTMagnetic field required for laser-assisted hyperpolarization
Clinical MRI Field Strength1.5 and 3TStandard magnets used in clinical imaging
Experimental MRI Field Strength7TMagnet used for signal comparison (Figure 1)
Nuclear Spin Coherence Time (T2)> 90sAchieved in bulk hyperpolarized solid (Reference 2)
Current MRI ResolutionMillimeter to CentimeterLength ScaleCurrent limitation in clinical practice
Target MRI ResolutionMolecularLength ScaleGoal for quantum-enhanced MRI
Diamond Phantom Inner Diameter2mmDimensions used in background suppression experiment
Diamond Phantom Outer Diameter4.2mmDimensions used in background suppression experiment

The dual-mode imaging technique relies on precise material engineering and quantum control protocols:

  1. Material Selection: Utilizing diamond microparticles or nanodiamonds specifically enriched with 13C isotopes to serve as the hyperpolarizable nuclear spin source.
  2. NV Center Creation: Engineering Nitrogen Vacancy (NV) centers—point defects consisting of a substitutional nitrogen atom adjacent to a lattice vacancy—to act as the spin-photon interface.
  3. Optical Excitation: Shining low-power laser light onto the diamond material to excite the NV centers, aligning their electron spins.
  4. Spin Transfer: Employing dynamic nuclear polarization (DNP) techniques to transfer the high electron spin polarization from the NV centers to the neighboring 13C nuclear spins.
  5. Dual Readout: Simultaneously acquiring high-resolution optical images (via NV fluorescence) and high-sensitivity MRI signals (via hyperpolarized 13C spins).
  6. Scaffolding Development (Future Work): Creating porous diamond structures (“diamond sponges”) to facilitate contact and subsequent spin transfer to external analytes (e.g., water, molecular markers) for in vivo applications.

6CCVD is uniquely positioned to supply the advanced MPCVD diamond materials required to replicate and extend this pioneering research in quantum sensing and enhanced imaging.

To achieve the high spin polarization and long coherence times necessary for quantum-enhanced MRI, researchers require highly specialized diamond substrates. 6CCVD offers:

Material SpecificationApplication Focus6CCVD Capability
Isotopically Enriched PCDBulk hyperpolarization, high-density 13C spin sources, porous scaffolds.MPCVD growth of Polycrystalline Diamond (PCD) enriched with 99.99% 13C for maximum nuclear spin density.
NV-Optimized SCD/PCDControlled NV center density for optimal spin-photon coupling.Custom nitrogen doping during growth or post-growth irradiation/annealing protocols to achieve desired NV concentrations.
High-Purity SCDFundamental physics, long coherence time (T2) studies, quantum computing.Single Crystal Diamond (SCD) plates with ultra-low native nitrogen (< 1 ppb) for superior spin coherence properties.
Boron-Doped Diamond (BDD)Electrochemical sensing and alternative hyperpolarization platforms.Custom BDD films and wafers available for exploring other hyperpolarized solid mechanisms (as mentioned in the paper).

The success of this research relies on precise material dimensions and surface quality, areas where 6CCVD excels:

  • Custom Dimensions: While the paper used microparticles, 6CCVD can supply large-area diamond wafers up to 125mm (PCD), which can be processed into high-volume microparticles or used as bulk substrates.
  • Precision Fabrication: We offer advanced laser cutting and etching services to create custom geometries, such as the specific 2mm/4.2mm ring structures used in the phantom experiments, ensuring high geometric accuracy for microfluidic integration.
  • Polishing Excellence: Achieving high-quality surfaces is critical for minimizing spin decoherence. 6CCVD guarantees ultra-smooth surfaces: Ra < 1nm for SCD and Ra < 5nm for inch-size PCD.
  • Metalization Services: For integrating diamond sensors into microwave (MW) loops or electronic readout systems (as shown in Figure 2), 6CCVD provides in-house metalization capabilities, including deposition of Au, Pt, Pd, Ti, W, and Cu films.

6CCVD’s technical sales team and in-house PhD material scientists are experts in tailoring MPCVD diamond growth recipes to meet specific quantum and biomedical requirements. We provide consultation on:

  • Optimizing 13C enrichment levels versus cost constraints.
  • Selecting the appropriate diamond grade (SCD vs. PCD) based on required coherence time and volume.
  • Developing custom metalization stacks for integration into complex Quantum Sensing and Dual-Mode Imaging devices.

For custom specifications or material consultation, visit 6ccvd.com or contact our engineering team directly.

View Original Abstract

His research team focuses on utilizing physical chemistry to develop “quantum-enhanced” NMR and MRI technologies, pushing past the current resolution and signal limitations.Beyond his research, Dr. Ajoy is very enthusiastic about his students and emphasizes the importance of the contributions made by his graduate and undergraduate researchers.Having become a professor during the SARS-CoV-2 pandemic, he is especially grateful for his students and expressed that the multiple papers published by his lab are due to the hard work of everyone on his team.Sophie Conti, one of Dr. Ajoy’s research assistants who works on the nitrogen vacancy center magnetometry in microfluidics project, said of the Ajoy lab, “I’ve really loved working in the Ajoy lab thus far because of the supportive community and amazing opportunities for learning.I think our lab is really unique in that undergraduates are really encouraged and supported by the other lab members to further their own learning and research if it interests them.” In this interview, we explore how the use of diamond microparticles can enhance MRI and optical imaging, resulting in a form of dual imaging that has revolutionary impacts for the fields of medicine, biology, and the physical sciences.