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Electrical Tuning of Tin-Vacancy Centers in Diamond

MetadataDetails
Publication Date2021-06-03
JournalPhysical Review Applied
AuthorsShahriar Aghaeimeibodi, Daniel Riedel, Alison E. Rugar, Constantin Dory, Jelena Vučković
InstitutionsStanford University
Citations31
AnalysisFull AI Review Included

Electrical Tuning of SnV Centers in Diamond: 6CCVD Technical Analysis

Section titled “Electrical Tuning of SnV Centers in Diamond: 6CCVD Technical Analysis”

This document analyzes the research demonstrating the electrical tuning of tin-vacancy (SnV) centers in single-crystal diamond (SCD) via the Stark effect. The findings are highly relevant for quantum network development, requiring ultra-high purity diamond substrates and advanced fabrication capabilities, which are core competencies of 6CCVD.


  • Core Achievement: Demonstrated reversible electrical tuning of SnV center optical transitions in SCD using the direct-current Stark effect.
  • Performance Metric: Achieved a tuning range exceeding 1.7 GHz, which is approximately 57 times the natural linewidth (~30 MHz).
  • Application Relevance: The tuning range is sufficient to overcome modest inhomogeneous detunings between distinct SnV emitters, enabling the realization of multiple identical quantum nodes.
  • Material Requirements: The experiment utilized electronic-grade, low-strain single-crystal diamond (SCD) to minimize native inhomogeneous broadening.
  • Defect Engineering: SnV centers were generated via 120Sn+ ion implantation (370 keV) followed by high-temperature vacuum annealing (up to 1100 °C).
  • Fabrication Complexity: Required precision nanostructuring (500-nm tall nanopillars/mesas) and custom metalization (5 nm Ti / 30 nm Au) for high-field electrode application.
  • Key Finding: Measured Stark coefficients ($\Delta\mu$ and $\Delta\alpha$) are several orders of magnitude smaller than non-inversion-symmetric color centers (e.g., NV-), confirming the SnV center’s high frequency stability.

The following hard data points were extracted from the research paper, focusing on material properties and experimental results.

ParameterValueUnitContext
Max Tuning Range> 1.7GHzAchieved via DC Stark effect
Tuning Factor~ 57TimesRelative to 30 MHz natural linewidth
SnV Linewidth (E1, zero field)194 ± 12MHzFull Width at Half-Maximum (FWHM)
SnV Center Wavelength ($\lambda_{C}$)619.254nmC transition, zero field
Ground State Splitting (GSS)819.6 to 989.4GHzRange observed across different SnV centers (E1-E4)
Implantation Ion120Sn+N/AUsed for SnV center generation
Implantation Energy370keVDetermines implantation depth
Expected SnV Depth~ 90nmBased on SRIM simulations
High Annealing Temperature1100°CVacuum anneal (90 minutes)
Quadratic Stark Coefficient ($\Delta\alpha / 4\pi\epsilon_{0}$)3.28 ± 0.18Å3E1 emitter (Predominantly quadratic shift)
Linear Stark Coefficient ($\Delta\mu$)3.9 ± 0.4 x 10-3DE2 emitter (Predominantly linear shift)
Electrode Gap1”mDistance between 4 ”m wide electrodes
Max Local Electric Field~ 50MV/mApplied across the electrodes

The experiment required precise control over material preparation, defect generation, and nanophotonic fabrication.

  1. Substrate Preparation: Electronic-grade, single-crystal diamond (SCD) was cleaned using a boiling tri-acid solution (1:1:1 sulfuric/nitric/perchloric acids).
  2. Surface Etch: The top 300 nm of diamond was removed using an oxygen (O2) plasma etch to prepare the surface.
  3. SnV Generation: 120Sn+ ion implantation was performed at 370 keV with a dose of 2 x 1011 cm-2, targeting a depth of approximately 90 nm.
  4. Defect Activation: Sequential vacuum annealing was conducted at 800 °C (30 minutes) and 1100 °C (90 minutes) to activate the SnV centers.
  5. Nanostructure Fabrication: Nanopillars and mesas (500 nm tall) were fabricated using e-beam lithography, a SixNy hard mask, and reactive ion etching (RIE) using SF6, CH4, and N2 gases.
  6. Electrode Metalization: Parallel electrodes (4 ”m wide, 1 ”m gap) were defined via e-beam lithography and metal liftoff. The metal stack consisted of 5 nm Titanium (Ti) followed by 30 nm Gold (Au), deposited via e-beam evaporation.
  7. Optical Characterization: Photoluminescence Excitation (PLE) measurements were performed at cryogenic temperatures (~5 K) while applying DC voltage (up to ±150 V) to the electrodes to measure the Stark shift.

6CCVD is uniquely positioned to supply the high-quality diamond materials and custom fabrication services required to replicate and advance this research in Stark tuning of Group-IV color centers.

Research Requirement6CCVD Solution & CapabilityTechnical Advantage
High-Purity SubstrateOptical Grade Single Crystal Diamond (SCD)SCD material with extremely low nitrogen content, minimizing background defects and ensuring the low-strain environment critical for achieving narrow SnV linewidths (194 MHz).
Custom Dimensions & ThicknessPlates/Wafers up to 125 mm; Thickness up to 500 ”mWe provide custom-sized SCD plates, ensuring optimal geometry for subsequent ion implantation and large-scale nanophotonic device fabrication.
Electrode IntegrationCustom Metalization Services (Ti/Au, Pt, Pd, W, Cu)We offer the precise 5 nm Ti / 30 nm Au metal stack used in the experiment, guaranteeing reliable, high-quality ohmic contacts necessary for applying high electric fields (up to 50 MV/m) without failure.
Surface Quality for NanostructuringUltra-Low Roughness Polishing (Ra < 1 nm)Our SCD surfaces are polished to Ra < 1 nm, which is essential for minimizing fabrication-induced strain and inhomogeneous broadening during the creation of 500-nm tall nanopillars.
Defect Engineering SupportConsultation on Implantation & AnnealingOur PhD engineering team assists researchers in optimizing material selection and post-growth processing recipes (e.g., 1100 °C vacuum annealing) to maximize SnV center yield and spectral stability.
Global Supply ChainGlobal Shipping (DDU default, DDP available)We ensure rapid and secure delivery of sensitive SCD materials to international research facilities, supporting time-critical quantum projects.

Optical Grade Single Crystal Diamond (SCD) is required to replicate the low-strain, high-purity environment necessary for SnV centers. For applications requiring high thermal conductivity or integration with complex electronics, 6CCVD can also provide Polycrystalline Diamond (PCD) substrates up to 125 mm in diameter.

6CCVD offers custom metalization services, including the specific Ti/Au stack used for the high-voltage electrodes, as well as precision laser cutting for unique chip dimensions required for nanophotonic integration. We can also supply substrates pre-thinned to specific depths, optimizing the material for subsequent ion implantation targeting shallow SnV centers (~90 nm).

6CCVD’s in-house PhD team specializes in defect engineering and can assist researchers in optimizing material selection, surface preparation, and post-growth annealing recipes for maximizing SnV center yield and minimizing strain in similar Stark Effect Tuning projects.

For custom specifications or material consultation, visit 6ccvd.com or contact our engineering team directly.

View Original Abstract

Group-IV color centers in diamond have attracted significant attention as solid-state spin qubits because of their excellent optical and spin properties. Among these color centers, the tin-vacancy (Sn-V<sup>-</sup>) center is of particular interest because its large ground-state splitting enables long spin coherence times at temperatures above 1 K. However, color centers typically suffer from inhomogeneous broadening, which can be exacerbated by nanofabrication-induced strain, hindering the implementation of quantum nodes emitting indistinguishable photons. Although strain and Raman tuning have been investigated as promising tuning techniques to overcome the spectral mismatch between distinct group-IV color centers, other approaches need to be explored to find methods that can offer more localized control without sacrificing emission intensity. Here, we study the electrical tuning of Sn-V<sup>-</sup> centers in diamond via the direct-current Stark effect. We demonstrate a tuning range beyond 1.7 GHz. We observe both quadratic and linear dependence on the applied electric field. Further, we also confirm that the tuning effect we observe is a result of the applied electric field and is distinct from thermal tuning due to Joule heating. Stark tuning is a promising avenue toward overcoming detunings between emitters and enabling the realization of multiple identical quantum nodes.