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Influence of the Characteristics of a Workpiece on the Slicing Characteristics Including Tool Wear

MetadataDetails
Publication Date2018-01-01
JournalMATEC Web of Conferences
AuthorsSatoshi Sakamoto, Masaya Gemma, Yasuo Kondo, Kenji Yamaguchi, Mitsugu Yamaguchi
InstitutionsYokohama National University, Yamagata University
Citations4
AnalysisFull AI Review Included

Technical Documentation & Analysis: Precision Slicing of Hard Materials

Section titled “Technical Documentation & Analysis: Precision Slicing of Hard Materials”

This document analyzes the findings of “Influence of the Characteristics of a Workpiece on the Slicing Characteristics Including Tool Wear” and connects the requirements for processing ultra-hard materials to the advanced capabilities offered by 6CCVD (6ccvd.com), a global leader in MPCVD diamond solutions.


This study provides critical insights into the relationship between workpiece mechanical properties (hardness and toughness) and the performance metrics of diamond multi-wire sawing, directly informing the processing requirements for advanced 6CCVD diamond materials.

  • Hardness vs. Slicing Time: Higher hardness and toughness (e.g., Sapphire, 23.0 GPa) significantly increase the required slicing time and accelerate diamond wire tool wear.
  • Accuracy Driver: Workpiece brittleness was found to adversely affect wafer thickness variation more than absolute hardness.
  • Toughness for Precision: Sapphire, possessing the highest toughness (2.1 MPa), exhibited the smallest wafer thickness variation, demonstrating that high toughness suppresses microfracture and wire wandering, leading to superior slicing accuracy.
  • Tool Wear: Significant abrasive fall-off and core wire damage were observed when slicing the hardest, toughest material (Sapphire), emphasizing the need for robust, high-quality diamond tools.
  • Chipping Control: The frequency of chipping depends primarily on workpiece hardness, while the size of chipping depends on workpiece toughness.
  • Methodology: Experiments utilized a diamond electrodeposited wire tool (143 ”m OD, 20-30 ”m grain size) running at 100 m/min with a fixed feed rate of 0.8 mm/min.

The following hard data points were extracted from the experimental setup and material characterization:

ParameterValueUnitContext
Wire Core Diameter100”mDiamond electrodeposited wire tool
Wire Outer Diameter143”mDiamond electrodeposited wire tool
Abrasive Grain Size20-30”mDiamond
Wire Running Speed100m/minReciprocating multi-wire saw
Wire Tension14.6NConstant tension setting
Workpiece Feed Speed0.8mm/minConstant feed rate
Coolant Supply Rate50mL/minGlycol-based water-soluble fluid
Sapphire Vickers Hardness23.0GPaHighest hardness tested
Sapphire Fracture Toughness2.1MPaHighest toughness tested
TEMPAX Slicing Time~20minShortest time (Lowest H/T)
Sapphire Slicing Time~50minLongest time (Highest H/T)
Chipping Measurement Threshold1.50”mMinimum size measured for analysis

The experimental investigation focused on controlled slicing parameters to isolate the influence of workpiece mechanical properties:

  1. Apparatus: A wire reciprocating type multi-wire saw was used, controlling feeding and rewinding via a single drum.
  2. Tool Specifications: A diamond electrodeposited wire tool was employed, featuring a 100 ”m core diameter, 143 ”m outer diameter, and a diamond grain size of 20-30 ”m.
  3. Workpieces: Four materials were tested: Borosilicate glass (TEMPAX), Single Crystal Silicon (Mono-Si), Polycrystalline Silicon (Poly-Si), and Sapphire. All samples were 20 mm x 20 mm x 5 mm.
  4. Kinematics: The wire running speed was fixed at 100 m/min, and the workpiece feed speed was fixed at 0.8 mm/min.
  5. Fluid Management: A glycol-based water-soluble coolant was supplied at a rate of 50 mL/min.
  6. Characterization: Slicing time, wafer thickness variation (measured at 11 points), surface quality (SEM), and tool wear (abrasive fall-off and core damage) were measured and correlated with Vickers hardness and fracture toughness values.

The research confirms that slicing ultra-hard, high-toughness materials like sapphire requires optimized processing and results in significant tool wear. As the manufacturer of the hardest material known (Diamond, > 90 GPa Vickers Hardness), 6CCVD provides the necessary SCD and PCD substrates and engineering expertise required for successful precision processing.

To replicate or extend this research—especially when moving to the ultimate hard material, diamond—6CCVD offers materials optimized for demanding slicing and subsequent device fabrication:

6CCVD MaterialApplication RelevanceKey Specification
Optical Grade SCDSubstrates for high-precision optical windows, quantum computing, or high-power electronics. Requires ultra-low damage slicing.Thickness: 0.1 ”m to 500 ”m. Polishing: Ra < 1 nm.
Electronic Grade PCDLarge-area heat spreaders or mechanical components where high hardness and large dimensions (up to 125mm) are critical.Custom Dimensions: Plates/wafers up to 125 mm. Polishing: Ra < 5 nm (Inch-size).
Heavy Boron Doped Diamond (BDD)Potential use in advanced electrodeposited wire tools or wear-resistant components, leveraging BDD’s conductivity and extreme hardness for enhanced tool life.Thickness: Up to 500 ”m. Available as wafers or custom shapes.

The study highlights the challenge of achieving low thickness variation and minimizing chipping size in hard materials. 6CCVD’s in-house capabilities ensure that the starting material is optimized for subsequent precision processing:

  • Custom Dimensions: While the paper used 20 mm x 20 mm samples, 6CCVD routinely supplies custom plates and wafers up to 125 mm in diameter (PCD) and large-area SCD, accommodating industrial-scale slicing requirements.
  • Ultra-Precision Polishing: The study noted that high toughness reduces surface damage. 6CCVD guarantees Ra < 1 nm for SCD, providing a superior starting surface that minimizes the need for aggressive post-slicing lapping and polishing.
  • Integrated Metalization: For applications where the sliced wafer requires subsequent device integration (e.g., electrodes or contacts), 6CCVD offers internal metalization services including Au, Pt, Pd, Ti, W, and Cu layers, applied directly to the SCD or PCD surface.
  • Substrate Thickness Control: We offer SCD and PCD substrates in precise thicknesses ranging from 0.1 ”m to 500 ”m, ensuring engineers can select the optimal starting material thickness to minimize waste during the high-wear slicing process.

The relationship between hardness, toughness, and slicing parameters is complex. 6CCVD’s in-house PhD team specializes in the mechanical and physical properties of CVD diamond. We offer consultation services to assist engineers and scientists in optimizing material selection and processing recipes for similar hard material slicing and processing projects, ensuring maximum yield and minimal tool wear.

For custom specifications or material consultation, visit 6ccvd.com or contact our engineering team directly.

View Original Abstract

Multi-wire saws with a diamond electrodeposited wire tool are widely used to slice hard and brittle materials. The properties of the materials significantly affect the saw’s performance in terms of slicing quality, efficiency, and accuracy. In this study, the effects of the material properties of workpieces on wire tool performance and tool wear are described. The main conclusions are as follows: the higher the hardness and toughness of the workpiece material, the longer the slicing time and greater the damage to the wire tool. The brittleness of the workpiece adversely affects the thickness variation more than its hardness. In addition, the frequency of chipping mainly depends on the hardness of the workpiece, whereas the chipping size mainly depends on the toughness of the workpiece.