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Diamond anvils probe the origins of Earth’s magnetic field

MetadataDetails
Publication Date2017-02-07
JournalProceedings of the National Academy of Sciences
AuthorsCharles Q. Choi
Citations2
AnalysisFull AI Review Included

6CCVD Technical Analysis: Diamond Anvils in Extreme High-Pressure Research

Section titled “6CCVD Technical Analysis: Diamond Anvils in Extreme High-Pressure Research”

This document analyzes the requirements for diamond materials used in high-pressure, high-temperature (HPHT) research, specifically focusing on Diamond Anvil Cells (DACs) utilized to simulate planetary core conditions. The findings directly inform material selection and customization services offered by 6CCVD.


The research highlights the critical role of high-quality, synthetic diamond in simulating the extreme conditions of Earth’s core (P > 1 million atmospheres, T > 4,000 K).

  • Core Application: Laser-Heated Diamond Anvil Cells (DACs) are essential tools for geophysicists studying the thermal conductivity of iron under extreme pressure.
  • Material Requirement: The diamond anvils must possess exceptional mechanical strength, chemical inertness, and high optical transparency to allow stable, uniform laser heating and precise optical probing.
  • Precision Challenge: Experiments require micron-scale samples and highly precise anvil geometry (flatness and centering) to prevent sample destruction via chemical reactivity or diffusion during laser exposure.
  • Contradictory Results: Current discrepancies in thermal conductivity measurements (a factor of three difference) underscore the need for improved experimental techniques, demanding higher material purity and geometric precision in the diamond anvils.
  • 6CCVD Value Proposition: 6CCVD specializes in providing high-purity, low-defect Single Crystal Diamond (SCD) tailored for DAC applications, offering custom dimensions, superior polishing (Ra < 1nm), and engineering support to optimize anvil performance.

The following hard data points were extracted from the analysis, defining the extreme operating environment for the diamond anvils:

ParameterValueUnitContext
Simulated Pressure> 1Million AtmospheresRequired to simulate Earth’s core conditions
Simulated Temperature> 4,000Kelvin (K)Required for laser heating of iron samples
Anvil ThicknessFewMillimetersStandard geometry for DAC anvils
Sample Size (Iron)Couple ofµmExtremely small scale requires high precision
High Thermal Conductivity Estimate~90Watts per meter per KelvinBased on electrical resistivity measurements
Low Thermal Conductivity Estimate18-44Watts per meter per KelvinBased on direct thermal diffusivity measurements
Required Surface Finish (Implied)Ra < 1nmNecessary for uniform heating and alignment

The research relies on advanced laser-heated DAC techniques, which place stringent demands on the diamond material and setup stability.

  1. Sample Encapsulation: Micron-sized iron samples are loaded into a pressure medium and placed between two SCD diamond anvils.
  2. Pressure Generation: Mechanical force is applied to the anvils to achieve pressures exceeding 1 million atmospheres.
  3. Laser Heating: Stable, high-power fiber lasers are directed through the transparent diamond anvils to heat the sample to extreme temperatures (>4,000 K).
  4. Geometric Control: Critical requirements include ensuring the anvils are perfectly centered and flat, and the sample chamber is free of impurities (e.g., water) to guarantee uniform heating and prevent sample destruction.
  5. Thermal Measurement (Method A - Electrical Resistivity): Iron wires are used to measure electrical resistivity, which is then correlated to thermal conductivity. This method is highly sensitive to sample irregularities.
  6. Thermal Measurement (Method B - Thermal Diffusivity): Heat pulses are applied, and the rate of heat propagation is measured by monitoring changes in the brightness and wavelength of light emitted from the sample.
  7. Stability Requirement: Laser pulses must be precisely controlled (not too long or too strong) to prevent chemical reactivity and diffusion within the sample and surrounding diamond material.

6CCVD is uniquely positioned to supply the high-specification MPCVD diamond materials necessary to advance HPHT research, addressing the current limitations related to material purity and geometric precision.

To replicate and extend this research, 6CCVD recommends Optical Grade Single Crystal Diamond (SCD).

6CCVD MaterialSpecificationRationale for DAC Application
Optical Grade SCD (Type IIa)Low nitrogen content, high purity, minimal defects.Ensures maximum optical transparency across a broad spectrum for laser heating and optical probing. Essential for stable operation at >4,000 K.
High-Strength SCD SubstratesThickness up to 500 µm (wafers) or 10 mm (substrates).Provides the necessary mechanical integrity to withstand pressures exceeding 1 million atmospheres without catastrophic failure.

The success of DAC experiments hinges on the precision of the anvil geometry, a core strength of 6CCVD’s manufacturing process.

  • Custom Dimensions and Thickness: 6CCVD can supply SCD plates and substrates up to 10 mm thick, allowing researchers to specify the exact anvil geometry (e.g., specific culet size, bevel angles, and thickness) required for their pressure range.
  • Ultra-Precision Polishing: We guarantee surface finishes critical for uniform heating and alignment.
    • SCD Polishing: Achievable surface roughness Ra < 1 nm. This level of flatness is crucial for ensuring uniform pressure distribution and preventing localized stress points that lead to early anvil failure or non-uniform sample heating.
  • Metalization Services: While the primary anvil is SCD, electrical resistivity measurements (Method A) often require integrated contacts. 6CCVD offers in-house deposition of standard metal stacks, including Ti, Pt, Au, Pd, and W, allowing for the creation of integrated electrical leads or heating elements directly on the diamond surface.

6CCVD’s in-house team of PhD material scientists specializes in optimizing diamond properties for extreme environments.

  • HPHT Geometry Optimization: We provide consultation on material selection and geometric design to maximize the lifespan and performance of diamond anvils under specific pressure and temperature profiles.
  • Defect Management: Our MPCVD process ensures low-defect SCD, minimizing internal stress points that could compromise the anvil’s integrity when subjected to multi-megabar pressures.
  • Material Consistency: We ensure batch-to-batch consistency, which is vital for replicating high-pressure experiments and resolving the current discrepancies observed between research groups.

For custom specifications or material consultation, visit 6ccvd.com or contact our engineering team directly.

View Original Abstract

Why is Earth covered by oceans and teeming with life, when Mars remains arid and apparently lifeless? The reasons are many, ranging from atmospheric characteristics to the planet’s distance from the Sun. But one key condition may involve the ability of the Earth’s core to generate a magnetic field.

Diamond anvils squeeze samples to extreme pressures while probing them with lasers directed through the diamonds. Geophysicists use the anvils to simulate the extreme pressures of the Earth’s interior. Image courtesy of Sergey Lobanov (Geophysical Laboratory, Carnegie Institution of Washington, Washington, DC).

And yet the origins of the Earth’s magnetic field remain a mystery for a variety of reasons. For one, there’s the small matter of accessing that chiefly iron core, which is buried under 1,800 miles of rock. This has left scientists resorting to lasers and diamond anvils in the laboratory to heat and squeeze iron to recreate the kind of temperatures and pressures found in the deep Earth. Thus far, these experiments have offered conflicting results, raising more questions than answers (1, 2).

Earth’s magnetic field is generated by its dynamo: the electrically conducting liquid metals in the planet’s outer core that churn or convect because of heat, like boiling water roiling in a pot. The strength of this convection depends on how much heat flows from the outer core to Earth’s mantle, which in turn depends on the thermal conductivity of iron and its alloys.

The planet, including its core, is cooling. If condensed-matter scientists can determine the present-day temperature of the Earth’s core and the thermal conductivity of iron, “we can estimate how …